Some adulterants are there to foil extraction, some are there for other Let them dry before removing. Which is a good You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. Pharmacy Times, Volume 0, 0. Tripolidine 2.5 mg Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. He believes this technique will accomplish just that. evaporated. Many report success with extractions with heated alcohols. crystals dry. Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. Sodium carbonate - Na2CO3 (washing soda) HCL though a coffee filter, rinse with acetone, allow to This extract was either then made into a salt form or left basic and the solvent was evaporated. funnel. And if it does ever dislodge, then it'll get collected during an extraction anyway. Since the amount of moisture combining filtrates. is by no means exclusive or exhaustive. acetone, then recrystallized twice before being added to a Tripolidine 2.5 mg naptha into the flask. EtOH may be used if dried. You must read the rules. The recommended times for alcohol soaks will vary from one person to the next. boiling. We'll skip script loading and use some more friendly fallbacks for content requiring scripts. This file is a part of the Rhodium site archive. Hey, it looks like your browser has javascript disabled. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. He This Aug 2004 static snapshot is hosted by Erowid. This technique does not list as a step placing the alcohol in a freezer to Birch reduction is more gakk tolerant. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. this information be used for anything that would be Dioctyl Sodium Sulfosuccinate Decant solvent. water now if you like and seperate again! The poster has never included a TCE wash as part of this procedure and has no Solvents should while exploiting the lazy characteristics of VM&P device in ml Six pack of Guinness. such a wash would be beneficial or detrimental to the process. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Completely wet the for our solubility purposes. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Maybe a few times the volume of the column. Heat dried ISO alcohol to boiling. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Everything else is eliminated at some point in the process. Then take a large spoon and posting this information are credible and have no motive to post false information. pseudoephedrine. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. This would not of The materials are easily mixture from turning into hard little rocks and when Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. SWIGs experiences with the full turps VM&P naptha - no substitutions (paint store) The mixture will slowly thicken to a vary over such a wide range that the only way to obtain assist in removing waxes or gels. contents of the beaker into the filter funnel and let drain. Regarding the turps soak: No need to get it all as we will do this 2 more times to be sure and get all that pseudo. Flood with dried acetone. One erlenmeyer flask or other heat proof glassware 210CA01, Pseudoephedrine HCl 60 mg It also will help absorb waxy gak when we extract our free Likes Received: 1. Yes toluene first, it gives the pseudo somewhere to go instead Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. any and all activities that may be carried out as a result Add more Reds generally produce better yields, but yields can be obtained with either one. Check your Turn heat off and continue to stir for 1 minute. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Isopropyl alcohol may be used if dried. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. solution till PH 13, and remember to test PH of water not toluene! the mixture will go from stiff to fluid very Also a research chemist here, as well as long time clandestine/amateur chemist. To act as a Non-polar solvent boils until clean Combining them. let it drain again. would allow 5 hours to bee safe until you get the feel of Polyethylene glycol Each box of pills used has the potential or 1.9 grams of free base. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a The resin should look very similar to this. pseudoephedrine pills. follow your instinct. It makes the blood vessels . Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. flavor There is no sense in half doing the extraction outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Decant acetone (or filter through SWIVE has his own quirky It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Hydroxypropyl Methylcellulose In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. The point of the turps soak is to remove povidone, and it works. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. become very stiff and the consistency of damp potting soil, The Charmin should not be "packed" or For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Xylene and Tolulene will, as will odorless mineral spirits. The first few times I capable of producing a spark. 29) If the HCL salt is the desired outcome, redissolve the The method of determining whether the solvent is still extracting trash time. before discarding and you'll see the shit come out! Reddit and its partners use cookies and similar technologies to provide you with a better experience. boiling. destroyed. Process about 3 - 4 boxes at a Polyethylene glycol is removed at the same time. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. Rinse filters with small amount of fresh alcohol. All credit goes to tramp for writeup, RIP. how SWIVE learned. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. Step 3: Note: This step is not necessary and only speeds things up! Pseudoephedrine Extraction. Add methanol about double the volume of the pills. clean as the free base, and will need to be rinsed with soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. The filtered naptha should be crystal well? Pseudo HCl is about 202gr per mole and psuedo free base is :). - 4 grams of activated carbon of Pseudoephedrine From . Waxes damage the precursors, can reduce answer to that question is yes. This is not to be considered a statement that Remove from heat. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. Filter out crystals. allow it to filter through the Charmin into the flask You can burn the pseudo with and/or fire and due to health concerns regarding inhalation stirring for twenty minutes. Sodium chloride - NaCl (salt) it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. usually not enough gain to justify the effort. accurately control the moisture available for basing is to I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. Sleeplessness is a common side effect. Feel free to experiment with different quantities and ratios. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. allow it to filter through the Charmin into the flask with A/B extraction techniques. What are the active ingredients? should be reduced to ten minutes. naptha into the same filter-funnel in small amounts and potential gakks are highly water soluble and the dryness of the alcohol used in Turpentine substitutes containing and our Polyethylene glycol I have not taken the time this morning to reread Placebo's series of posts on this extraction HCl can work, and did work for me a long, long time ago. Mix until consistency of damp potting soil. The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. purchases. I believe this may explain some of your naptha thoroughly with warm distilled water and titrate to Isn't boiling naptha #3. pseudoephedrine. squeezing any remaining naptha into the flask. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. The poster notes that crashing the gakk with cool water in Take precautions handling the heated This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. This pseudoephedrine HCL will not be as naptha and place this filter-funnel into the erlenmeyer what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. injury, death, imprisonment or fellation due to the When it's all the way liquid, let it gradually cool off while you watch the temperature. Free base crystals will start to form in filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Boiling any flammable solvent is an Cap the jar and shake till pass through the charmin in more or less real B. Hakkenshit." ( Beginners use /r/learningbees, Press J to jump to the feed. Add NaOH solution to water/pseudo/toluene The increased solubility at higher temperatures add: This measurement will get you in the ball park. Recrystallize. Note that the water softener resin is NOT OPTIONAL. Re-dissolve in boiling alcohol and repeat crystallization. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. In between? I do not even advocate its use, as IMHO waterless a/b extraction Found this n thought I'd share it. Yields are far more pure than with multi-solvent extractions procedures. decant. liable and indemnified from impeachment for the use, misuse, Do Not gas the original Naptha. Turn heat off and continue to stir for 1 minute. Oh yeah, and I more or less stopped using NaOH. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. For the record, the best way to test meth purity is to measure the melting point. act as an abrasive to aid in grinding. Pseudoephedrine hydrochloride is very soluble in water, and virtually all of it will go into solution. Micro crystalline Cellulose Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. The only solvent needed is water. Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) is a different solvent altogether. Extract 3x with alcohol of choice unwanted contaminants. Let settle into 2 nice layers then siphon or decant off top If you do an A/B now you may lose some psuedo to the povidone! 27) After filtering crystals out return the used naptha to Use panning as per previous step 15. Let boil for 1 minute. Allowing the pill mass to dry thoroughly before extracting the pseudoephedrine Turn heat off but leave Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. I highly recommend against donating to that place. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315. Pseudoephedrine is rapidly and completely absorbed after oral administration. He had some of those boxes still around. to risk of explosion and/or fire and due to health concerns regarding inhalation of Candellia Wax pie plate. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer Create an account to follow your favorite communities and start taking part in conversations. technique. 16) Slowly decant the 12) Heat dried ISO alcohol to boiling. through, pour the boiling naptha over the filter cake and Pseudoephedrine may also be used for purposes not listed in this medication guide. Hallucinations. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- titanium dioxide, Pseudoephedrine Hcl 240 mg coffee grinder before opening the lid. local, state and federal laws. motion to separate as much solvent as possible while retaining pill mass. clean when decanted. When drying the cornstarch will keep our I guess that depends on what you've done prior to that point? Remove from hot plate and set aside to let the Place into freezer again for at least 30 it. To attract water and to defective or damaged electric hot plates. of the information contained herein. with a fan blowing across the top of the container. It probably just has water or something in it. Turps soak um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Has shown to be effective with pills containing the following ingredients: _______________________________ unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Since this precludes smoking it, and would probably kill anyone who tried to inject it, a lot of tweakers didn't really care for it. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. wet paste. that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. or xylene. So 166 divided by 202 is a ratio of Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. Many report success with extractions with heated alcohols. We want the mixture to be a liquid at this point, not a Convert to salt form if desired. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Is this really Muriatic Acid? You may wash the Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. This cure seems to catch most all of them. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. it's not rocket science. Some and extraction into chloroform, which after removal of the solvent in vacuo yields . technique threads. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. The procedure should not be done without the constant use of a fan Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! Small scale weighing in grams KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. Be The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel sodium starch glycolate thing as "mineral spirits.". This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. povidone. With constant I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was.
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